Good news! The cleaner, the better! Spooked by impurities!
"... used electron microscopy to directly verify that trace amounts of oxygen in the samples were indeed causing the spurious charge-order signal. ...
Not only has the team identified a crucial difference between cuprate and nickelate superconductors; they now have a more reliable method for growing cleaner samples that can potentially be used for a wider variety of experiments, with a little less mystery. ..."
From the abstract:
"A hallmark of many unconventional superconductors is the presence of many-body interactions that give rise to broken-symmetry states intertwined with superconductivity. Recent resonant soft X-ray scattering experiments report commensurate 3a0 charge density wave order in infinite-layer nickelates, which has important implications regarding the universal interplay between charge order and superconductivity in both cuprates and nickelates. Here we present X-ray scattering and spectroscopy measurements on a series of NdNiO2+x samples, which reveal that the signatures of charge density wave order are absent in fully reduced, single-phase NdNiO2. The 3a0 superlattice peak instead originates from a partially reduced impurity phase where excess apical oxygens form ordered rows with three-unit-cell periodicity. The absence of any observable charge density wave order in NdNiO2 highlights a crucial difference between the phase diagrams of cuprate and nickelate superconductors."
Fig. 4: Outline of the multistage reduction process of nickelate films and high-resolution STEM images of a partially reduced film showing 3a0 ordering.
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